Generation of copper nanoparticles by electro-exploding wire technique for various pressures of the surrounding medium

نویسندگان

  • Rashmita Das
  • Basanta Kumar Das
  • M. V. Suryanarayana
  • M. Sankari
  • Archana Sharma
چکیده

This paper presents the experimental results on explosion of copper wire at a discharge voltage of 9kV for the generation of Cu nanoparticles in nitrogen environment at different pressures. The current and voltage waveforms for different pressures of the nitrogen gas have been recorded by a current transformer and a high voltage probe. Nanoparticles generated by the electro exploded wire method were characterized by both optical microscopy and transmission electron microscopy. Experiments show that the variation of pressure of nitrogen gas inside the exploding chamber determines the size of the particles formed during the explosion of the copper wire. It is observed that for a pressure of less than 230 mbar of nitrogen gas, the wire does not explode and the copper wire remains intact. Micro particle generation occurred at a pressure of 2.3×10 2 mbar of nitrogen gas and nanoparticles were formed when the pressure was further increased to 1×10 3 mbar. Experimental results show that we could deposit maximum energy into the metal core when the wire was exploded by working in the high pressure regime of the nitrogen gas resulting in the production of nanoparticles. Transmission electron microscopy reveals the size of the nanoparticles to be in the range of 35 to 75 nm.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Synthesis of Cu-CuO and Cu-Cu2O Nanoparticles via Electro-Explosion of Wire Method

   We report an investigation on the synthesis of Copper Oxide nanostructures via the Electro-Explosion of Wire method. Cu-CuO and Cu-Cu2O nanoparticles with mean particle size of 21.1 to 59.1 nm were synthesized by changing the applied current density and amount of used Tetra Methyl Ammonium Hydroxide as the surfactant. The X-ray diffraction analysis, field emission scanning ele...

متن کامل

Fluorescence from metallic silver and iron nanoparticles prepared by exploding wire technique

The observation of intense visible fluorescence from silver and iron nanoparticles in different solution phases and surface capping is reported here. Metallic silver and iron nanoparticles were obtained by exploding pure silver and iron wires in pure water. Bovine serum albumin protein adsorption on the silver nanoparticles showed an enhanced fluorescence. The presence of polyvinyl pyrrolidone ...

متن کامل

Surface Modification of Glassy Carbon Electrode by Ni-Cu Nanoparticles as a Competitive Electrode for Ethanol Electro-Oxidation

In the present study, Nickel-Copper nanoparticles were electrodeposited on glassy carbon electrode (GCE) by using electroplating deposition method. The prepared electrode was characterized by scanning electron microscopy (SEM) and elemental mapping analysis. Results showed that Ni-Cu nanoparticles with a high density are distributed at the surface of the glassy carbon electrode. Subsequentl...

متن کامل

Application of copper oxide nanoparticles modified glassy carbon electrode for electrocatalytic oxidation of methanol

Copper nanoparticles were fabricated by electro-reduction of CuSO4solution in the presence of cetyltrimethylammonium bromide (CTAB) cationic surfactant as an additive through potentiostatic method. The prepared copper nanoparticles were characterized by scanning electron microscopy (SEM) and electrochemical methods. The SEM images reveal that the nanoparticles with diameters at about 70 n...

متن کامل

A Review of Methods for Synthesis of Al Nanoparticles

The synthesis of metallic nanoparticles is an active area of academic and, more significantly, applied research in nanotechnology. Several methods have been introduced for the synthesis of these materials. The techniques for synthesizing aluminum nanoparticles can be divided into solidphase, liquid-phase and gas-phase processes. The solid-phase techniques include mechanical ball milling and mec...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2017